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Method to Recover Media Ligand Losses During Sorption of Rare Earth Elements from Simulated Geothermal Brines

This document describes the method and results of an in-situ experiment used to confirm that ligand bleed from a sorptive media can be contained. The experiment focused on maintaining the media's sorption of rare earth elements (REE) obtained from a simulated geothermal brine dop...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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Column Sorption Uptake and Regeneration Study; Rare Earth Element Sorbent Uptake and Sorbent Stripping

Study of rare earth element (REE) uptake from geothermal brine simulant by column loading, metal recovery through stripping, and regeneration of column for re-loading. Simulated brine testing.
Lanyk, T. Tusaar Corp.
Dec 18, 2015
3 Resources
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Experimental Parameters Affecting Stripping of Rare Earth Elements from Loaded Sorptive Media in Simulated Geothermal Brines

Experimental results from several studies exploring the impact of pH and acid volume on the stripping of rare earth elements (REEs) loaded onto ligand-based media via an active column. The REEs in this experiment were loaded onto the media through exposure to a simulated geother...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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Sorption Capacity of Europium for Media 1 and Media 2 from Solution at Ambient Temperature

This dataset shows the capacity for Europium of media #1 and media #2 in a shakertable experiment. The experimental conditions were 150mL of 500ppm Eu solution, 2g of media, pH of 3.2, at ambient temperature.
Garland, G. Tusaar Corp.
Mar 16, 2015
2 Resources
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Dynamic Column Extraction for Europium on Media 1 at Ambient Temperature

This is a dataset for a 200ppm europium solution sent through a column with 12g of media #1 at pH of 3.2. This column experiment was run at ambient temperature at a flow rate of 2mL/min.
Garland, G. Tusaar Corp.
Apr 07, 2015
2 Resources
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Repetitive Regeneration of Media 1 after REE Sorption from Brine 1 at 70C

This dataset shows the ability of media #1 to be loaded with REE's, stripped of the REE's sequestered, regenerated, and reused over many cycles.
Garland, G. Tusaar Corp.
Jul 23, 2015
3 Resources
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Improved Rare Earth Element Sorption from Simulated Geothermal Brines: Effect of Gassed versus Degassed Brines

A study exploring sorption and stripping characteristics of sorption media when simulated geothermal brines are degassed or not degassed. Experiments were done at 70degC. The brines used in this study were formulated by Tusaar. The two brines used/simulated are labeled 1M and 1C...
Stull, D. Tusaar Corp.
May 24, 2016
2 Resources
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REE Sorption Study of Seived 50 +100 Mesh Fraction of Media 1 in Brine 1 at Different Concentrations of REE at 70C

This dataset shows the sorption capacities of smaller grain size (-50 +100 mesh) of media #1 in brine #1 at different starting concentrations of REE's at elevated temperature of 70C. The experimental conditions are 2g of 50 +100 mesh media #1 to 150mL of REE solution at concentrat...
Garland, G. Tusaar Corp.
Jun 29, 2015
4 Resources
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Shaker Table Experiments with Rare Earth Elements Sorption from Geothermal Brine

This dataset described shaker table experiments ran with sieved 50 +100 mesh media #1 in brine #1 that have 2ppm each of the 7 REE metals at different starting pH's of 3.5, 4.5, and 5.5. The experimental conditions are 2g media to 150mL of REE solution, at 70C.
Garland, G. Tusaar Corp.
Jul 21, 2015
4 Resources
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Repetitive Regeneration of Media #1 in a Dynamic Column Extraction using Brine #1

This data is from a regeneration study from a dynamic column extraction experiment where we ran a solution of REE's through a column of media #1 then stripped the REE's off the media using 2M HNO3 solution. We then re-equilibrated the media and repeated the process of running a RE...
Garland, G. Tusaar Corp.
Oct 14, 2015
4 Resources
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Rare Earth Element Sorption Study on sieved 50 +100 mesh fraction of Media 1 in Brine 1 with Different Starting pHs at 70C

This is a continuation of the rare earth element sorption study for shaker bath tests on 2g media #1 in 150mL brine #1 with different starting pH's at 70C. In a previous submission we reported data for shaker bath tests for brine #1 with starting pH's of 3.5, 4.5 and 5.5. In this ...
Garland, G. Tusaar Corp.
Sep 29, 2015
5 Resources
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Retrospective Analysis of Geothermal Mineral Recovery and Domestic Resource Assessment References

This reference database in RIS format contains all of the references that were collected as part of our retrospective analysis of geothermal mineral recovery (REE and Li) activities and domestic resource assessment. The outputs detail the chemistry and molecular processes used in ...
Dobson, P. and Stringfellow, W. Lawrence Berkeley National Laboratory
Oct 20, 2021
4 Resources
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Manganese Uptake of Imprinted Polymers

Batch tests of manganese imprinted polymers of variable composition to assess their ability to extract lithium and manganese from synthetic brines at T = 45 deg C . Data on manganese uptake for two consecutive cycles are included.
Ventura, S. SRI International
Sep 30, 2015
1 Resources
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Lithium Uptake Data of Lithium Imprinted Polymers

Batch tests of lithium imprinted polymers of variable composition to assess their ability to extract lithium from synthetic brines at T = 45 degC. Initial selectivity data are included
Ventura, S. SRI International
Dec 04, 2015
1 Resources
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Lithium and Manganese Uptake Data from Initial Set of Imprinted Polymers

Batch tests of cross-linked lithium and manganese imprinted polymers of variable composition to assess their ability to extract lithium and manganese from synthetic brines at T=45 deg C .
Ventura, S. SRI International
Mar 27, 2015
1 Resources
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RN12 and RN30 Epidote anlayses

Results for laser ablation measurement of rare earth elements and electron microprobe analysis of major elements in hydrothermal epidote. Laser ablation measurements were completed using an Agilent 7700 quadrupole ICP-MS coupled with 193nm Photon Instruments Excimer laser.
Fowler, A. and Zierenberg, R. University of California
Jan 01, 2015
1 Resources
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Recovery of Rare Earths, Precious Metals and Other Critical Materials from Geothermal Waters with Advanced Sorbent Structures

The work evaluates, develops and demonstrates flexible, scalable mineral extraction technology for geothermal brines based upon solid phase sorbent materials with a specific focus upon rare earth elements (REEs). The selected organic and inorganic sorbent materials demonstrated h...
Addleman, R. et al Pacific Northwest National Laboratory
Sep 30, 2015
2 Resources
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Advanced Sorbent Structure Recovery of REEs, Precious Metals and Other Valuable Metals from Geothermal Waters and Its Associated Technoeconomics

This work evaluates, develops and demonstrates flexible, scalable mineral extraction technology for geothermal brines based upon solid phase sorbent materials with a specific focus upon rare earth elements (REEs). The selected organic and inorganic sorbent materials demonstrated h...
Addleman, S. et al Pacific Northwest National Laboratory
May 25, 2017
3 Resources
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Gd Uptake Experiments for Preliminary Set of Functionalized Adsorbents (With Content Model)

These data summarize adsorption experiments conducted with Gd in 0.5 M NaCl. Results represent preliminary, proof-of-concept data utilizing fine-powder silica gel as the adsorbent support. Future testing will focus on larger, application-appropriate beads.
Noack, C. Carnegie Mellon University
Jul 01, 2015
1 Resources
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Simbol Materials Lithium Extraction Operating Data From Elmore and Featherstone Geothermal Plants

The data provided in this upload is summary data from its Demonstration Plant operation at the geothermal power production plants in the Imperial Valley. The data provided is averaged data for the Elmore Plant and the Featherstone Plant. See average brine composition tab for submi...
Harrison, S. Simbol, Inc
Jul 01, 2015
1 Resources
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Rare Earth Element Content of Thermal Fluids from Surprise Valley, California

Rare earth element measurements for thermal fluids from Surprise Valley, California. Samples were collected in acid washed HDPE bottles and acidified with concentrated trace element clean (Fisher Scientific) nitric acid. Samples were pre-concentrated by a factor of approximately 1...
Fowler, A. and Zierenberg, R. University of California
Sep 23, 2015
1 Resources
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Brine Stability Study

This is a study of the brine formulations that we were using in our testing were stable over time. The data includes charts, as well as, all of the original data from the ICP-MS runs to complete this study.
Garland, G. Tusaar Corp.
Apr 15, 2015
6 Resources
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REE Sorption Study for Media #1 and Media #2 in Brine #1 and #2 at different Liquid to Solid Ratio's at Ambient Temperature

This data set shows the different loading capacities of Media #1 and Media #2 in a high and low salt content brine matrix at different liquid to solid ratio's. These data sets are shaker bath tests on media #1 and media #2 in brine's #1 and #2 at 500mL-.5g(1000-1 ratio), 150mL-.75...
Garland, G. Tusaar Corp.
Mar 27, 2015
9 Resources
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Techno-Economic Assessment for Integrating Biosorption into Rare Earth Recovery Process

The current uncertainty in the global supply of rare earth elements (REEs) necessitates the development of novel extraction technologies that utilize a variety of REE source materials. Herein, we examined the techno-economic performance of integrating a biosorption approach into ...
Jiao, Y. et al Lawrence Livermore National Laboratory
Jul 01, 2017
1 Resources
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Chelating Resins for Selective Separation and Recovery of Rare Earth Elements from Low Temperature Geothermal Water

Study on the use of organic ligands to extract lanthanides from low temperature geothermal water.
Callura, J. Carnegie Mellon University
Dec 31, 2016
1 Resources
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